ANALYTICAL CHEMISTRY II

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Learning Outcomes

Will explain the basic terms used in volumetric titrimetry.
Explains titration.
Defines standard solution.
Defines equivalence point.
Defines endpoint.
Defines primary standard.
Will explain the titration of a strong acid with a strong base.
Solves strong acid-strong base problems.
Draws the strong acid-strong base titration curve.
Will explain the titration curves of weak acids.
Solves weak acid-strong base problems.
Draws the weak acid-strong base titration curve.
Will explain the titration curves of weak bases.
Solves weak base-strong acid problems.
Draws the weak base-strong acid titration curve.
Will explain the properties of polyprotic acids and bases.
Explains the concept of polyprotic acid.
Lists polyprotic acids.
Explains the concept of polyprotic base.
Lists polyprotic bases.
Will explain the titration curves in polyprotic systems.
Solves titration problems in polyprotic systems.
Draws the titration curve in polyprotic systems.
Will explain the applications of neutralization titrations.
Lists primary standard substances used in acid standardization.
Lists primary standard substances used in base standardization.
Explains the steps of elemental analysis.
Explains the Kjeldahl method.
Explains the saponification reaction.
Will explain the titration curves in complexometry.
Explains the endpoint of complexometric titration.
Explains the complex constant.
Will explain the calculations in complexometric titration.
Calculates the donor amount.
Calculates the complex constant.
Will explain the titration curves in precipitation titrations.
Explains the endpoint of precipitation titration.
Identifies relevant data for the solubility product (Ksp) of the precipitating compound.
Will explain the calculations in precipitation titration.
Performs quantitative analysis of the precipitating compound.
Calculates the Ksp of the precipitating compound.
Will explain redox reactions.
Defines the components of electrochemical cells.
Identifies the species in the reaction according to their electronegativity.
Writes the half-reactions.
Balances redox reactions.
Will explain the structures of electrochemical cells.
Identifies the anode/cathode reactions.
Classifies electrochemical cells.
Defines electrodes according to their uses.
Writes the schematic representation of cells.
Writes the resulting cell reaction.
Will explain electrode potentials.
Explains cells based on standard electrode potentials.
Interprets the signs of electrode potentials.
Explains the role of the standard hydrogen electrode.
Will explain the Nernst equation.
Writes the Nernst equation for half-reactions.
Calculates the potentials for half-reactions.
Will explain the electrochemical cell potentials.
Calculates electrode potentials.
Classifies the cell according to the calculated electrode potential.
Writes the cell reaction according to the calculated electrode potential.
Calculates electrode potentials using activities.
Will explain the redox equilibrium constants.
Writes the equilibrium constant expression for redox reactions.
Calculates the equilibrium constant for redox reactions.
Will explain redox titrations.
Distinguishes species that affect the medium potential in redox titrations.
Calculates the cell potential before the equivalence point.
Calculates the cell potential at the equivalence point.
Calculates the cell potential after the equivalence point.
Will explain potentiometry.
Explains the general principles of potentiometry.
Lists and explains the structures of electrodes used in potentiometry.
Explains how direct potentiometry is used.
Explains potentiometric pH measurements using a glass electrode.
Lists the errors that affect pH measurements.
Explains how potentiometric titrations are performed.
Draws potentiometric titration curves.
Explains potentiometric determination of equilibrium constants.
Solves problems related to potentiometric applications.
Will explain conductometry.
Explains the general principles of conductometry.
Explains Ohm’s law.
Lists the forces acting on ions in a solution.
Explains the structure of a conductometer.
Draws conductometric titration curves.
Solves problems related to conductometric applications.
Will explain electrogravimetry.
Explains the general principles of electrogravimetry.
Defines ohmic potential.
Explains polarization effects.
Distinguishes between two-electrode and three-electrode systems.
Will explain coulometry.
Explains the general principles of coulometry.
Calculates the charge transferred under constant current and time.
Lists and explains the types and characteristics of coulometric methods.
Explains coulometric titration applications.
Will explain the classification of separation techniques.
Explains why separation techniques are used.
Classifies separation techniques.
Explains the differences between separation techniques.
Will explain size-based separations.
Classifies filtration techniques.
Explains filtration techniques.
Defines dialysis method.
Classifies dialysis methods.
Will explain mass and density-based separations.
Explains centrifugation method.
Classifies centrifugation techniques.
Defines centrifugation applications.
Will explain phase change-based separations.
Explains distillation.
Explains sublimation.
Explains crystallization.
Will explain chemical state change-based separations.
Explains precipitation.
Explains volatilization.
Explains electrodeposition.
Will explain masking methods.
Explains complex formation.
Lists its applications.
Will explain phase distribution.
Explains the basic principles of extraction.
Classifies extraction methods.
Explains the Craig method.
Defines chromatography.
Classifies chromatographic methods.
Will explain column chromatography.
Defines column chromatography.
Defines the components of column chromatography.
Can set up a column chromatography system.
Will explain liquid chromatography.
Defines liquid chromatography.
Explains the application features of liquid chromatography.
Explains and distinguishes liquid-liquid and liquid-solid chromatography.
Will explain the structure of the liquid chromatography instrument.
Explains the working principles of the instrument.
Lists the parts of the instrument.
Explains the characteristics of the parts of the instrument.
Explains the functions of the parts of the instrument.
Will explain the detectors used in liquid chromatography.
Distinguishes between liquid chromatography detectors.
Explains the working principles of detectors.
Determines the type of detector based on the analyte type.
Will explain the columns and stationary phases in liquid chromatography.
Distinguishes between column types.
Explains the column fillings and separation properties.
Explains the factors affecting separation.
Determines the column type based on the analyte type.
Will explain qualitative and quantitative analyses using liquid chromatography.
Explains how qualitative analysis is performed.
Explains how quantitative analysis is performed.
Lists the variables that affect analysis results.
Will explain gas chromatography.
Defines gas chromatography.
Explains the application features of gas chromatography.
Explains and distinguishes between gas-liquid and gas-solid chromatography.
Will explain the structure of the gas chromatography instrument.
Explains the working principles of the instrument.
Lists the components of the instrument.
Explains the features of the instrument components.
Explains the functions of the instrument components.
Will explain the detectors used in gas chromatography.
Distinguishes between gas chromatography detectors.
Explains the working principles of detectors.
Determines the type of detector based on the analyte type.
Will explain the columns and stationary phases in gas chromatography.
Distinguishes between column types.
Explains the column fillings and separation properties.
Explains the factors affecting separation.
Determines the column type based on the analyte type.
Will explain qualitative and quantitative analyses using gas chromatography.
Explains how qualitative analysis is performed.
Explains how quantitative analysis is performed.
Lists the variables that affect analysis results.
Applies qualitative and quantitative analysis techniques to simple examples.
Will explain paper chromatography.
Defines a paper chromatography setup.
Creates a paper chromatography setup.
Performs a paper chromatography analysis.
Lists the variables affecting analysis results.
Evaluates the analysis results.
Will explain thin layer chromatography (TLC).
Defines a TLC setup.
Creates a TLC setup.
Performs a TLC analysis.
Lists the variables affecting analysis results.
Evaluates the analysis results.
Will explain the basic principles of electrophoresis.
Classifies electrophoretic methods.
Explains the basic principles of electrophoresis methods.
Explains electrophoretic movement.
Will explain paper and gel electrophoresis.
Explains the working principles of paper and gel electrophoresis.
Explains the use of gel electrophoresis in protein, DNA, and RNA analysis.
Will explain capillary electrophoresis.
Explains the separation principles in capillary electrophoresis.
Explains the basic principle of electroosmotic flow.
Interprets the factors affecting electroosmotic flow.
Will explain the structure of the capillary electrophoresis instrument.
Explains the working principles of the instrument.
Lists the components of the instrument.
Explains the types of capillary electrophoresis.
Lists the types of detectors used in capillary electrophoresis.
Will explain the applications of electrophoretic methods.
Explains the application areas of different electrophoretic techniques.
Evaluates the role of electrophoresis in pharmaceutical and biochemical analysis.
Will explain the basic concepts of quantitative analysis.
Explains quantitative analysis.
Explains the objectives of quantitative analysis.
Explains the fundamental analytical techniques used in quantitative analysis.
Explains the key terms in quantitative analysis.
Defines the basic laboratory materials used in quantitative analysis.
Will explain the basic procedures.
Prepares a solution with a known concentration and volume from a liquid standard substance.
Prepares a solution with a known concentration and volume from a solid standard substance.
Will explain volumetric titration.
Uses a burette.
Uses a pipette.
Selects an indicator.
Performs a titration.
Determines the endpoint.
Will explain the preparation of the secondary standard (base) solution.
Weighs the primary standard substance.
Selects the appropriate indicator.
Selects the appropriate indicator.
Prepares the secondary standard (base) solution with the primary standard substance.
Calculates the concentration of the secondary standard (base) solution.
Will explain the preparation of the acid solution.
Uses the secondary standard solution as a titrant.
Selects the appropriate indicator.
Prepares the acid solution using the secondary standard solution.
Calculates the concentration of the acid solution.
Will explain the quantitative determination of acidic analytes.
Evaluates the basic chemical properties of the acidic analyte.
Selects the appropriate indicator.
Titrates the acidic analyte with the secondary standard solution.
Calculates the concentration of the acidic analyte.
Will explain the quantitative determination of basic analytes.
Evaluates the basic chemical properties of the basic analyte.
Selects the appropriate indicator.
Performs a back titration.
Titrates the acidic analyte with the secondary standard solution.
Calculates the concentration of the basic analyte.
Will explain complexometry.
Explains the method of complexometry.
Recognizes chelating agents.
Prepares a solution of ethylenediaminetetraacetic acid.
Adjusts the ethylenediaminetetraacetic acid solution.
Performs stoichiometric calculations.
Will explain complexometric calcium determination.
Writes the reaction equation.
Titrates the calcium sample with ethylenediaminetetraacetic acid solution.
Calculates the concentration of calcium in the sample.
Will explain complexometric magnesium determination.
Writes the reaction equation.
Titrates the magnesium sample with ethylenediaminetetraacetic acid solution.
Calculates the concentration of magnesium in the sample.
Will explain precipitation titrations.
Explains the principles of precipitation titrations.
Classifies the indicator methods used in precipitation titrations.
Distinguishes the solubility products of the formed precipitates.
Will explain the Mohr method.
Explains the Mohr method.
Lists the application areas of the Mohr method.
Will explain chloride determination using the Mohr method.
Prepares and adjusts a silver nitrate solution.
Writes the reaction equations.
Titrates the chloride sample with silver nitrate using the Mohr method.
Performs a control experiment.
Calculates the concentration of chloride ions in the sample.
Will explain permanganometry.
Explains permanganimetry.
Balances the permanganimetric reaction equation.
Prepares a potassium permanganate solution.
Adjusts the potassium permanganate solution.
Performs stoichiometric calculations.
Will explain the permanganometric determination of hydrogen peroxide.
Writes the reaction equation.
Titrates the hydrogen peroxide sample with adjusted potassium permanganate solution.
Performs stoichiometric calculations and calculates the sample concentration.
Will explain the permanganometric determination of iron sulfate.
Writes the reaction equation.
Titrates the iron sulfate sample with adjusted potassium permanganate solution.
Performs stoichiometric calculations and calculates the sample concentration.
Will explain iodimetry.
Explains iodimetry.
Balances the iodimetric reaction equation.
Prepares an iodine solution.
Adjusts the iodine solution.
Performs stoichiometric calculations.
Will explain the iodimetric determination of ascorbic acid.
Writes the reaction equation.
Titrates the ascorbic acid sample with adjusted iodine solution.
Performs stoichiometric calculations and calculates the sample concentration.
Will explain the iodimetric determination of sodium thiosulfate.
Writes the reaction equation.
Titrates the sodium thiosulfate sample with adjusted iodine solution.
Performs stoichiometric calculations and calculates the sample concentration.
Will explain potentiometric measurements.
Sets up a potentiometric measurement setup.
Performs a potentiometer calibration.
Measures the pH with a potentiometer.
Prepares the potentiometer for reuse.
Will explain the quantitative determination using potentiometric titration.
Sets up a potentiometric titration setup.
Performs a potentiometric titration.
Quantitatively evaluates the potentiometric titration results.
Will explain the pKa determination using potentiometric titration.
Sets up a potentiometric titration setup.
Performs a potentiometric titration.
Determines the pKa from potentiometric titration results.
Will explain conductometric measurements.
Sets up a conductometric measurement setup.
Performs a conductometer calibration.
Measures conductivity with a conductometer.
Prepares the conductometer for reuse.
Will explain quantitative determination using conductometric titration.
Sets up a conductometric titration setup.
Performs a conductometric titration.
Quantitatively evaluates the conductometric titration results.
Will explain the preparation of conditions for UV-Visible spectroscopy.
Determines the appropriate conditions for the assay.
Selects the wavelength for the assay by obtaining the spectrum of the solution.
Will explain quantitative determination using UV-Visible spectroscopy.
Plots the working graph.
Creates the regression equation.
Calculates the amount of the target compound in the pharmaceutical product using the regression equation.
Determines the quantity using the Lambert-Beer law.
Will explain the preparation of experimental conditions for column chromatography.
Sets up the column chromatography setup.
Prepares the sample for analysis.
Will explain the separation of dyes using column chromatography.
Applies the samples to the column chromatography setup.
Separates the dye substances by collecting different fractions.
Will explain the preparation of experimental conditions for HPLC.
Prepares the mobile phase.
Prepares the instrument for analysis.
Prepares the sample for analysis.
Will explain the analysis of samples using HPLC.
Applies the samples to the HPLC instrument.
Performs the analysis.
Will explain the evaluation of HPLC analysis results.
Qualitatively evaluates the analysis results.
Quantitatively evaluates the analysis results.
Will explain the preparation of experimental conditions for gas chromatography.
Prepares the instrument for analysis.
Prepares the sample for analysis.
Will explain the analysis of samples using gas chromatography.
Applies the samples to the gas chromatography instrument.
Performs the analysis.
Will explain the evaluation of gas chromatography analysis results.
Qualitatively evaluates the analysis results.
Quantitatively evaluates the analysis results.
Will explain the qualitative determination of components using TLC.
Sets up the TLC setup.
Applies the samples to the TLC setup.
Qualitatively evaluates the TLC results.
Will explain the quantitative determination of components using TLC.
Sets up the TLC setup.
Applies the samples to the TLC setup.
Quantitatively evaluates the TLC results.